張加研, 吳春華, 秦永劍, 王家學(xué)( 西南林學(xué)院木質(zhì)科學(xué)與裝飾材料工程學(xué)院,云南昆明650224)
摘 要:以甲醇、50%甲醇、70 %丙酮及50 %丙酮等為溶劑,石油醚為沉淀劑從思茅松樹(shù)皮中提取了寡聚原花色素。以寡聚原花色素標(biāo)準(zhǔn)品為對(duì)照,比較了提取物與標(biāo)準(zhǔn)品的紅外光譜,并通過(guò)紫外光譜法對(duì)提取物中寡聚原花色素的含量進(jìn)行了測(cè)定,結(jié)果表明:上述溶劑均可從思茅松樹(shù)皮中提取寡聚原花色素,提取率分別為1.08 %、1.41 %、1.78 %和2.53 %。
關(guān)鍵詞:思茅松樹(shù)皮;寡聚原花色素;提取
中圖分類(lèi)號(hào):TQ91 文獻(xiàn)標(biāo)識(shí)碼:A 文章編號(hào):1673-5854(2007)01-0034-03
A Preli minary Study on Extraction of Oligomeric Proanthocyanidins from the Bark of Simao Pine
ZHANG Jia-yan,WU Chun-hua,QIN Yong-jian,WANG Jia-xue
( Faculty of Wood Science and Decoration Engineering,Southwest Forestry Kollege,Kun ming 650224,China)
Abstract: Oligomeric proanthocyanidins(OPCs) were prepared from the bark of Simao pine by extraction with solvents such as methanol,50% methanol,70% acetone and 50% acetone,and precipitation of petroleum ether. The extracts were compared with the OPCs reference material from Tianjin Jianfeng Company by IR spectrum. The OPCs contents in extracts were deter mined by UV method. The results showed that the OPCs could be extracted from Simao pine bark with all above solvents. The extraction yield was 1.08 %,1.41 %,1.78 % and 2.53 %,respectively.
Key words: bark of Simao pine;oligomeric proanthocyanidians;extraction